Wet Milling for Micronization in API Development stand

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Wet Milling for Micronization in API Development

When discussing “Wet-Mill Micronization” in API (Active Pharmaceutical Ingredient) development, we’re talking about a process used to reduce the particle size of the API within a liquid environment.1 Here’s a breakdown:

Wet-Mill Micronization:

  • Purpose:
    • The goal is to decrease the particle size of the API, which can significantly impact its solubility, dissolution rate, and bioavailability. This is crucial for ensuring the drug works effectively.
    • It also aids in creating a more uniform particle size distribution, leading to consistent dosing in the final drug product.4
  • Process:
    • Unlike dry millingwet milling involves suspending the API in a liquid medium.
    • Particle size reduction is achieved through forces like shearing, impact, and crushing, often using equipment with Wahals’ rotor-stator systems and/or Wahal ZR SPlash bead mills in series .
    • This method is particularly useful for APIs that are sensitive to heat or static charge, which can be issues in dry milling.

Role of Tip Speed:

  • Impact on Performance:
    • “Tip speed” refers to the velocity of the rotor’s edge in a wet mill. It’s a critical parameter influencing the amount of shear force applied to the API particles.
    • Generally, higher tip speeds result in greater shear forces, leading to finer particle size reduction.
    • Therefore, by adjusting the tip speed, Wahal can fine-tune the particle size distribution of the API.
    •   quality.
    • The tip speed has a strong influence on the amount of energy that is transferred to the product being milled. Therefore it is a very important parameter in the milling process.

In essence, tip speed is a key operational parameter in wet milling that directly affects the efficiency and outcome of the micronization process.

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